In the meanwhile, the effects of varied acids for protecting third carbonyl group were investigated. Through the trial and error, the mixture of anhydrous alcohol/ petroleum benzine is the good solvent of target molecule recrystal.
考察了酸性对保护3位羰基的影响,确定了无水乙醇/石油醚是目标分子重结晶的最佳溶剂体系。
Method s: Soxhlet extractor was previously applied to grape seeds for the remover of oils with petroleum benzine.
方法:对新疆葡萄酒厂废渣中葡萄籽用石油醚脱脂,脱脂后的葡萄籽用乙醇提取。
Compared with the traditional process, yield of diosgenin was raised by 25.1 percent, the consumption of hydrochloric acid reduced by 90%, and the consumption of petroleum benzine decreased by 60%, and the production was much purer.
该工艺同传统提取工艺相比:皂素收率的提高率为25.1%;产品纯度高;盐酸用量降低90%以上,石油醚用量降低了60%以上。
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